Mercury Pycnometery Testing Vs. Mercury Porosimetry Testing: What’s the Difference?
In Mercury
Porosimetry testing, the pressure is actually applied to force mercury into smaller
and tinier pores. Hence, the pore size distribution can be anticipated by measuring
applied pressure and the intrusion volume in the test using Mercury
Porosimeter.
With its unlimited
user-defined data-points, automated data collection, and reduction, Mercury
Porosimeter is the ultimate porosimeter available in the market. This
engineering instrument is automated, and versatile machinery used to regulate
innumerable properties.
It
basically allows mercury porosimetry testing under higher or lower temperatures
to put on concrete operational conditions.
On the
contrary,
For
Mercury Pycnometery Testing, a mercury pycnometer is used to precisely gauge the
extents of particles or solid samples with a volume of less than 0.1
cm>s3/sup. PMI’s Mercury Pycnometer is user-friendly, delivers accurate outcomes
in less than 10 minutes, and accommodates an extensive range of samples.
The
pycnometer consists of a glass flask with a close-fitting ground glass stopper
with a vessel hole through it. This fine hole emits excess liquid after closing
a top-filled pycnometer and allows obtaining a specified volume of measured
and/or working fluid with high precision.
Mercury Porosimetry Testing vs.
Mercury Pycnometery Testing: An Overview
Mercury
porosimetry testing is an operational technique used to analyze porosity, pore
size distribution, and volume to represent an inclusive range of powder and
solid materials.
The
instrument, known as a porosimeter, effectively imposes a pressurized chamber
to force mercury to intervene into the vacuums in a porous substrate. As
pressure is placed, mercury fills the larger pores first. As pressure rises,
the filling arises to tinier pores.
The
inter-particle pores between the individual particles and the intra-particle
pores within the particle can be categorized using this testing method.
Whereas Pycnometery Testing is usually carried out for comparing
and measuring densities or explicit gravities of liquids and solids, including
soil.
The powder’s
pycnometer density offers the hypothetical density of the powder and can also deliver
a hint of issues with internal voids within a powder.
For instance,
if a drop of pycnometer density is detected either within particle size cuts or
lot, the expected cause could be internal voids due to the fabrication
technique.
Furthermore,
the pycnometer density also provides a practical test to evaluate the powder
for any gross changes from lot to lot.
Salient
Features of Mercury Pycnometery Testing Equipment
•
Mercury
Test Substance
•
Length
of test around 10 minutes
•
Wide
range of adequate sample types and sizes
•
Minimal
maintenance required
•
Bulk
Density: Pore Structure Characteristics
Specifications
of Mercury Pycnometery Testing Equipment
Sample Size |
1 inch D x 1.5 inch H |
Pore Size Range |
0 – 15 microns |
Determined Pressure |
Vacuum – 1 Atm |
Power Requirements |
110/220VAC, 50/60 Hz |
Reproducibility |
More than 0.5% |
Salient Features of Mercury Porosimetry
Testing Equipment
·
Completely
automatic and user- friendly
·
Windows-based
software handles all control, statistics collection, measurement, and report
generation
·
manual
control
·
Software
upgrades for more than 3 years
·
Limitless
user-defined data points based on volume, pressure, or a combination
·
Comes
with real-time graphical test display with up-to-date configuration
·
Computer
equipped program depicts testing status and results during operation
·
Demonstrates
both intrusion and extrusion curve
·
A
broad range of adequate sample sizes and types
·
Requires
minimal maintenance
·
Low
level of mercury exposure
·
Sample
transfers from low pressure to high-pressure stations not required
·
Non-destructive
testing
Specifications
of Mercury Porosimetry Testing Equipment
Pore Diameter Range |
0.003 – 350 µm |
Pressure Range vacuum |
up to 60,000 psi |
Pressure Transducers |
low, medium, and high ranges |
Sample Size |
25mm diameter and 25mm long |
Examination Ports |
2 low- and high-pressure ports |
Sample Volume |
up to 10 cc or more |
Pressurizing Fluid |
mercury |
Vacuum Pump |
two-stage, direct-drive rotary oil pump |
Permeability Range |
1×10-4 – 5 Darcy |
Pressurizing Gas |
clean, dry, or compressed air any other non-flammable and non-corrosive gas |
Weight |
150 kg |
Resolution |
1 in 60,000 |
Accuracy |
0.15% of reading |
Power Requirements |
230 VAC, 50Hz |
Pressure Range |
0 -200 psi |
Final Words,
Mercury porosimetry
testing is essentially used to examine porosity, pore size distribution, and
volume. While Pycnometery Testing is carried out for measuring and comparing
densities liquids and solids.
Both types
of tests are conducted by Mercury Pycnometery Tester and Mercury Porosimetry
Tester designed for such testing procedures.
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